In this work NMR techniques, 1D and 2D, are used for identification of aroma precursors, in particular glycosilate terpenes, in grape juice. The focus of this work is to find an analytical way to determine these precursors in a complex matrix like wine or juice and improve the poor knowledge about this particular kind of molecules. After using experiments like COSY, NOESY, TOCSY, HMBC, HMQC and others, nine molecules have been found in a sample of wine, previously separated in fractions by HPLC; some of these molecules seem to have never been discovered before, like a compound which contains the terpene 1,2-dihydroxylinalool.

Applicazione di tecniche di risonanza magnetica nucleare per l'identificazione di precursori d'aroma del vino nell'uva moscato giallo

Mazzaretto, Ivan
2012/2013

Abstract

In this work NMR techniques, 1D and 2D, are used for identification of aroma precursors, in particular glycosilate terpenes, in grape juice. The focus of this work is to find an analytical way to determine these precursors in a complex matrix like wine or juice and improve the poor knowledge about this particular kind of molecules. After using experiments like COSY, NOESY, TOCSY, HMBC, HMQC and others, nine molecules have been found in a sample of wine, previously separated in fractions by HPLC; some of these molecules seem to have never been discovered before, like a compound which contains the terpene 1,2-dihydroxylinalool.
2012-07-12
157
NMR, grape juice, terpene, linalool derivatives, glycosides, apiose
File in questo prodotto:
File Dimensione Formato  
Mazzaretto_tesi.pdf

accesso aperto

Dimensione 2.27 MB
Formato Adobe PDF
2.27 MB Adobe PDF Visualizza/Apri

The text of this website © Università degli studi di Padova. Full Text are published under a non-exclusive license. Metadata are under a CC0 License

Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/20.500.12608/15568